
nReminder of (forgotten) procedures
nGeneral rules
nProblems
Work safely
=
Work cleanly
=
Work accurately
Safety in the lab

‘Small accidents’
n2-Cyclohexene-1-one
nBalance
nGloves + rinsed


n24h => Anti-gif, doctors
nFlammazine
nInfection => antibiotics
+ corticoids
+ corticoids
nHyperpigmentation + allergy?
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Safety spectacles + lab coat

nALWAYS!


Lab tables
nSpace/clean

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Lab tables
nSpace/clean
nLabel name + date
http://www.biw.kuleuven.be/ifc/cok/intern/forms.htm
http://www.biw.kuleuven.be/ifc/cok/intern/forms.htm


Lab tables
nSpace/clean
nLabel name + date
nPlace back bottles


Lab tables
nSpace/clean
nLabel name + date
nPlace back bottles
nWhenever volatile products: FUME CUPBOARDS!


Lab tables
nSpace/clean
nLabel name + date
nPlace back bottles
nWhenever volatile products: FUME CUPBOARDS!
nSolvent-waste bottles: FUME CUPBOARDS!
Or closed!
Or closed!


Lab tables
nSpace/clean
nLabel name + date
http://www.biw.kuleuven.be/ifc/cok/intern/forms.htm
http://www.biw.kuleuven.be/ifc/cok/intern/forms.htm
nPlace back bottles
nWhenever volatile products: FUME CUPBOARDS!
nSolvent-waste bottles: FUME CUPBOARDS!
nClose fume cupboards


Balances

*Precision instrument!
nHorizontal
nSpace
nClean

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Waste disposal:
1.Needles
1.Needles

nDo not place back needle cap!
nRemove needle with red lid of yellow plastic box
nSyringe in contaminated waste

Waste disposal:
2. GC-vials
2. GC-vials

nRemove from tray after analysis!

Waste disposal:
2. GC-vials
2. GC-vials
nRemove from tray after analysis!
nSpecial box


Waste disposal:
2. GC-vials
2. GC-vials
nRemove from tray after analysis!
nSpecial box


Waste disposal:
2. GC-vials
2. GC-vials

nRemove from tray after analysis!
nSpecial box
nResults not interesting?

Waste disposal:
3. Pasteurpipettes
3. Pasteurpipettes
nContaminated waste


Waste disposal:
4. Product bottles
4. Product bottles
nRinse + dry +
remove cap
remove cap
nLab 02.92 (new)
nWrite down (also when bottle remains used!)

Plastic bottles
+ glass bottles
+ glass bottles
Broken glass

Waste disposal:
5. Chemicals
5. Chemicals
nLiquids: in barrels
nMore information?
=> Lieve
=> Lieve


Waste disposal:
5. Chemicals
5. Chemicals
nPowders: in special box


Waste disposal:
5. Chemicals
5. Chemicals
nContaminated waste: in special box


Dust masks

nWhenever powders
nSpecial gas masks:
outside labs (mind filter colour!)
outside labs (mind filter colour!)
–CO!

Gloves
nWhenever needed
nGreen rubber!



Dish washer
nDuty list:
Remind eachother !
Remind eachother !
nUse rubber gloves
nNo ‘spuwpotjes’
nGlassware should be precleaned:
–NO scrubbing machine
–NO products left


Centrifuge

nLeave it clean!

Miscellaneous I

nNever work ALONE in the lab!
nGas connections: check leaks!
nTap connections
nFume cupboard lab book
nRespect eachother’s set-ups
nRespect reservations (forms!)

Miscellaneous II
nHF: written authorisation!
nAvoid ovens to evaporate
nReport defects (lab responsible, technician, supervisor)
nLiquid nitrogen (gloves!)
nStoring samples (ask lab responsible, technician, supervisor)
nGeneral lab cleanings

nForms
4 General safety in the lab

Emergency procedures
nCall Emergency number
nFire:
1. Call ‘Fire!’
If people around: -> 2
If no one around: activate alarm, then -> 2
If people around: -> 2
If no one around: activate alarm, then -> 2
2. 1 attempt to exstinguish the fire (time!)
3. Call 997
4. If successful: wait for rescue team
If not successfull:
- activate alarm
- activate alarm
- go to ‘verzamelpunt’
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Evacuations
nContinuous siren (+/- 5 min)
>< test or automatic detection of fume,…= short pulse (3 seconds)
-> meant to activate EIP (first intervention team = Hugo + Johan M.)
-> they have 3 minutes to decide
‘accept’ (-> continuous siren -> general evacuation) or
‘decline’ (-> silence)
-> meant to activate EIP (first intervention team = Hugo + Johan M.)
-> they have 3 minutes to decide
‘accept’ (-> continuous siren -> general evacuation) or
‘decline’ (-> silence)
nSwitch off electric equipment
n(PC, printer can remain switched on)
nLeave lights on
nBring experiments in a ‘safe’ mode
nClose windows and doors
nLeave the building (take jacket, wallet, bag,…)
nDo not use the elevator!
nGo to reunion point (in front of main entrance of the building) and await further instructions
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